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Single Crystal X-Ray Diffractometer

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Single Crystal X-Ray Diffractometer at USIC

Requisition forms

Please download the requisition form, fill it in, sign it, and upload the filled copy with your booking. This requisition form is provided by the USIC office for this instrument.

Download requisition form PDF

Process: submit booking β†’ in-charge approval β†’ pay on the DU fee portal β†’ upload Order ID + receipt β†’ measurement confirmed. See the payment flowchart and user guidelines.

Booking details

Per sampleβ€”
Total costβ€”

Rates as per the revised USIC user-charges document β€” external rates include 18% GST. Per-hour instruments: enter the number of hours; per-sample instruments: number of samples.

Upload the filled & signed copy of the downloaded requisition form. Only genuine PDF files up to 5 MB are accepted.

Payment is mandatory with every booking. Pay the fee at the DU fee portal β€” fee.du.ac.in β†’ Fee Payment (Miscellaneous) β€” selecting β€œUSIC Instrumentation Fee” under the Fee dropdown. Then enter the Order ID and upload the fee receipt below β€” bookings without payment details are not accepted.

By submitting you accept the USIC user guidelines. Charges are payable in advance and non-refundable.

For any query related to the instrument
Contact: Mr. Sanjay (9568365216)

About this instrument

Make & Model: Rigaku Oxford Diffraction, XtaLAB Synergy-S

Key Instrument Features:

  • X-ray Source: PhotonJet Mo, Ceramic Fine Focus
  • X-ray Detector: HyPix-6000HE, Hybrid Pixel 2D detector
  • Cryojet System: 90 K – 300 K temperature range
  • Scanning Speed Range: 0.005–3.0Β°/sec
  • Sample Holder: Quartz capillaries (0.2, 0.3, 0.5 and 0.7 mm outer diameter)
  • Resolution:
    • 001Β° for Omega & Theta
    • 003Β° for Kappa
    • 005Β° for Phi
  • Generator: SPELLMAN DE60N 63 kV, 4.2 kW
  • Software: CrysAlisα΅–Κ³α΅’ for data collection and processing
  • Minimum Crystal Size: >0.1 mm