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Atomic Force Microscope (AFM)

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Atomic Force Microscope (AFM) at USIC

Requisition forms

Please download the requisition form, fill it in, sign it, and upload the filled copy with your booking. This requisition form is provided by the USIC office for this instrument.

Process: submit booking → in-charge approval → pay on the DU fee portal → upload Order ID + receipt → measurement confirmed. See the payment flowchart and user guidelines.

Booking details

Per sample—
Total cost—

Rates as per the revised USIC user-charges document — external rates include 18% GST. Per-hour instruments: enter the number of hours; per-sample instruments: number of samples.

Upload the filled & signed copy of the downloaded requisition form. Only genuine PDF files up to 5 MB are accepted.

Payment is mandatory with every booking. Pay the fee at the DU fee portal — fee.du.ac.in → Fee Payment (Miscellaneous) — selecting “USIC Instrumentation Fee” under the Fee dropdown. Then enter the Order ID and upload the fee receipt below — bookings without payment details are not accepted.

By submitting you accept the USIC user guidelines. Charges are payable in advance and non-refundable.

For any query related to the instrument
Contact: Mr. Lucky (8988263467)

About this instrument

The “Surfmera VEGA-PROXIMA AFM” is a fully automated atomic force microscope with ultimate stability and resolution for industrial and research applications. It supports large samples up to 200 × 200 mm and offers high-accuracy positioning, low noise, and advanced AFM mode in a single system.

1. Electronics & Software

1.1. Signal Processing:

  • Up to 24 scan channels
  • 512 Mb buffer; multiple high-speed FPGAs & DSP processors

1.2. Lock-in & Signal Generation:

  • 2 × analog lock-in amplifiers
  • 3 × digital lock-in amplifiers (supporting multifrequency modes)
  • 6 × 32-bit digital generators with advanced modulation options

1.3. Voltage Supplies:

  • ±10 V for independent tip and sample bias
  • ±150 V (optional) for extended bias experiments

1.4. Software & Automation:

  • Autofocus (laser/cantilever/sample), automated multiple area scanning
  • Optical + AFM image overlay and panoramic optical view  

2. Scanner & Positioning

2.1 Scanner (tip-scanning):

  • Type: Tube scanner with closed-loop sensors (XYZ)
  • Scan range (standard): 100 × 100 × 10 µm (XYZ)
  • Closed-loop: XYZ for all directions
  • Drive electronics noise: < 5 µV/√Hz

2.2 Sample Positioning (Motorized Stage):

  • Moving range: 200 × 200 mm in XY, 30 mm in Z
  • Positioning accuracy: ~1 µm (XY) and 0.2 µm (Z)
  • Thermal drift (stage): < 0.2 nm/min
  • Positioning speed: ~8 mm/s in XY
  • Navigation: Automated by video image or user-defined scanning scenario

3. Core AFM Modes

3.1. Contact & Static Modes

  • Contact AFM – Topography: Surface height mapping in direct contact.
  • Lateral Force Microscopy (LFM): Maps friction or lateral forces on surface.
  • Force Modulation: Mechanical property contrast via modulated contact force.
  • Spreading Resistance Imaging (SRI): Conductivity/resistance contrast in
    contact.
  • Piezoresponse Force Microscopy (PFM): Mapping ferroelectric domains and
    domain boundaries

3.2. Amplitude Modulation & Dynamic Modes

  • Amplitude Modulation (AM) AFM – Topography: Tapping (intermittent
    contact) imaging.
  • Phase Imaging: Tracks cantilever phase shift for material contrast.
  • Feedback Channel Scanning: Maps feedback signal for improved detail.

3.3. Electrical & Electrostatic Modes

  • Kelvin Probe Force Microscopy (KPFM)
  • Single- and two-pass
  • Amplitude & phase modulation modes

3.4. Electrostatic Force Microscopy (EFM)

  • Single- and two-pass
  • Amplitude & frequency modulation

3.5. Scanning Capacitance Force Microscopy (SCFM)

  • Single- and two-pass
  • dC/dZ and dC/dV capacitance imaging

These modes allow mapping of surface potential, charge distributions, and dielectric properties at the nanoscale.

3.6. Magnetic Force Microscopy (MFM)

  • Two-pass lift modes
  • Frame lift DC/AC magnetic contrast imaging

Used for magnetic domain structures, thin magnetic films, and data storage materials.

3.7. Spectroscopy & Force Curves

  • Force–Distance Spectroscopy – Force curves vs separation
  • Amplitude–Distance & Phase–Distance Spectroscopy
  • I(V) and I(Z) – Current vs bias and height curves

3. Nanolithography

  • Voltage-driven lithography
  • Current-driven lithography
  • Force-driven lithography

Supports patterning and modification of surfaces at the nanoscale.

4. Sample Requirement: The sample must be a completely dry, thin film synthesized using
an appropriate scientific method.