Nuclear Magnetic Resonance (NMR) Liquid State

Spectroscopy Facilities

Make: Jeol, Model: JNM-ECZ 400S
Specifications: 400 MHz
Observable Nuclei: Multinuclear, Full range
1 H, 13 C, 19 F all nuclei between 15N-31P
Stability 0.1 Hz/hour ( 2 H internal lock used)
Standard frequencies: 1 H : 400 MHz, 13 C:100 MHz
Variable temp. Facility: -140 to 180° C
Gradient strength: 0.3T at 10Amp setting
Auto sampler capacity 64 samples
Sound proof air compressor

For any query related to the instrument,
Contact : Mr. Dheeraj (8384079733)

Category Spectroscopy Facilities
Availability Available
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Instrument's Description

The Nuclear Magnetic Resonance spectroscopy is vital for both organic and inorganic chemists for structure elucidation on a routine basis and to follow reactions and dynamic chemical events on a real time scale.

Sample Description

The sample must be sufficiently soluble in a deuterated solvent to yield an NMR spectrum.
 For 1 H NMR, it is recommended to dissolve between 2 and 10 mg in 0.6 to 1 mL of solvent so that the sample depth is at least 4-4.5 cm in the tube.
 For 13 C NMR between 10 and 50 mg of sample is recommended.
 Too concentrated a solution sometimes leads to lower resolution. If sample or solubility is limited, it may still be possible to obtain a spectrum on the 500 MHz spectrometer. The choice of solvent is dictated by various factors such as viscosity, spectral interference, boiling point, and, of course, cost.

Price List

For Internal usage Per Sample of Carbon	20
For Internal usage Per Sample of Proton	10
For External (Academics) usage Per Sample of Carbon	500
For External (Academics) usage Per Sample of Proton	250
For External (Industries) usage Per Sample of Carbon	600
For External (Industries) usage Per Sample of Proton	400